Cyclohexanone → Bicyclohexyl

HRID 2100221

Reaction equation

HRID 2100221 reaction equation
[OH-].[K+].[C:3]1(=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>>[CH:3]1([CH:3]2[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]2)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1

Participants

3

Reactant 2

HCID 7967CyclohexanoneHCID 14797Potassium Hydroxide

Product 1

HCID 7094Bicyclohexyl

Procedure

140 g KOH (solid) are added to 2,000 g (20.41 mol) cyclohexanone. The mixture is heated under reflux with stirring. After 0.5 h, the reaction is terminated. The mixture is analyzed by GC analysis.

Workup

  1. temperatureThe mixture is heated
  2. temperatureunder reflux
  3. customthe reaction is terminated

Sources & evidence

ORD record
ord-b064e21093e544a1be1db11e8bf7d415
Source dataset
uspto-grants-2009_08
Patent number
US07572435B2

Linked notes

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