Ethyl bromopyruvate → HCID 7171906, compound

HRID 2107281

Reaction equation

HRID 2107281 reaction equation
[CH2:1]([NH:4][C:5]([NH2:7])=[S:6])[CH:2]=[CH2:3].Br[CH2:9][C:10](=O)[C:11]([O:13][CH2:14][CH3:15])=[O:12]>C(O)C>[CH2:1]([NH:4][C:5]1[S:6][CH:9]=[C:10]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[N:7]=1)[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 66144Ethyl bromopyruvateHCID 1549517Allylthiourea

Product 1

HCID 7171906HCID 7171906, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The reaction described in Preparation 42 was repeated but using 20 g of allylthiourea, 37 g of ethyl bromopyruvate and 200 ml of ethanol, giving the title compound as a pale yellow powder.

Workup

  1. customThe reaction described in Preparation 42

Sources & evidence

ORD record
ord-0e9e1c5001ae40ca92cf91cc4ae3ef25
Source dataset
uspto-grants-1990_06
Patent number
US04933355

Linked notes

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