3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide → Benzamide

HRID 2109247Notes

Reaction equation

HRID 2109247 reaction equation
C1(N2C(C(C)C)=C(C=O)C=N2)CC1.N([C:17]1[CH:18]=[C:19]([CH:40]=[CH:41][C:42]=1C)[C:20]([NH:22]C1C=C(C(C)(C)C)C=C(NS(C)(=O)=O)C=1OC)=[O:21])=[N+]=[N-]>>[C:20]([NH2:22])(=[O:21])[C:19]1[CH:40]=[CH:41][CH:42]=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 210792023-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamideHCID 210972411-Cyclopropyl-5-isopropyl-1H-pyrazole-4-carbaldehyde

Product 1

HCID 2331Benzamide

Procedure

Example 75 benzamide was prepared from 1-cyclopropyl-5-isopropyl-1H-pyrazole-4-carbaldehyde and 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide in the same manner as Example 39. ESI MS m/z 606 [C31H39N7O4S+H]+.

Sources & evidence

ORD record
ord-077ee128ab5b48dea962928c97af6f9e
Source dataset
uspto-grants-2009_04
Patent number
US07514458B2

Reaction notes

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