Acetyl chloride → HCID 22751291, compound
Reaction equation
C(Cl)(=O)C.[C:5](Cl)(=[O:9])[O:6][CH2:7][CH3:8].[C:11]1([CH:17]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH2:18][C:19]2[NH:20][CH2:21][CH2:22][N:23]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[CH2:7]([O:6][C:5]([N:23]1[CH2:22][CH2:21][N:20]=[C:19]1[CH2:18][CH:17]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)=[O:9])[CH3:8]Participants
4
Procedure
In place of acetyl chloride in Example 53, ethyl chlorocarbonate was reacted with 2-(2,2-diphenyl ethyl)-2-imidazoline to give 1-ethoxycarbonyl-2-(2,2-diphenyl ethyl)-2-imidazoline having a melting point of 78° to 80° C.
Sources & evidence
- ORD record
- ord-77220b60a0c5414e99669de5ad350c36
- Source dataset
- uspto-grants-1979_01