Ethanol → HCID 70600924, compound
Reaction equation
C([O:4][CH2:5][CH2:6][C:7]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)([OH:9])[CH3:8])(=O)C.[OH-].[Na+].C(O)C>O>[C:11]1([C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=1[C:7]([OH:9])([CH3:8])[CH2:6][CH2:5][OH:4]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 2.84 g. of 1-acetoxy-3-p-biphenylyl-3-butanol and 2 g. of NaOH in 30 ml. of 80% ethanol is boiled for 3 hours. Water is added and the mixture is extracted with chloroform and the extract is evaporated to give 3-p-biphenylyl-1,3-butanediol, m.p. 115°-117°.
Workup
- extractionthe mixture is extracted with chloroform
- customthe extract is evaporated
Sources & evidence
- ORD record
- ord-383f8c73496d4930845867d6bce64886
- Source dataset
- uspto-grants-1979_01
- Patent number
- US04136200
Reaction notes
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