4-Chlorobenzoyl chloride → N'-t-butyl-N'-(4-chlorobenzoyl)hydrazine

Reaction equation

[C:1]([N:5]([C:7](=[O:14])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[NH2:6])([CH3:4])([CH3:3])[CH3:2].[Cl:15]C1C=CC(C(Cl)=O)=CC=1>>[C:1]([N:5]([C:7](=[O:14])[C:8]1[CH:9]=[CH:10][C:11]([Cl:15])=[CH:12][CH:13]=1)[NH2:6])([CH3:4])([CH3:2])[CH3:3]

Participants

Reactant 2

HCID 85014-Chlorobenzoyl chloride

HCID 1275961N-(tert-butyl)benzohydrazide

Product 1

HCID 15617780N'-t-butyl-N'-(4-chlorobenzoyl)hydrazine

Procedure

N'-t-butyl-N'-(4-chlorobenzoyl)hydrazine was prepared substantially according to the procedure for preparing N'-t-butyl-N'-benzoylhydrazine described for Example 220, Step 3, except 4-chlorobenzoyl chloride was used in place of benzoyl chloride.

Sources & evidence

ORD record: ord-c1cb0b2079b34ecfbc7b20278066af92
Source dataset: uspto-grants-1995_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05424333

Reaction notes

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