HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenecarbodithioic acid → Bis(thiobenzoyl) Disulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenecarbodithioic acid | HCID 67141 | — |
| Reactant | Potassium triiodide | HCID 105053 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Bis(thiobenzoyl) Disulfide | HCID 10902862 | — |
Reaction Steps
100 ml of a sodium salt solution of dithiobenzoic acid (0.15 mol) were added by drops to an 80 not iodine aqueous solution (0.1 mol) over 1 hour. After completing the reaction, the obtained product was dissolved in an organic solvent of tetrahydrofurane (THF) and washed with distillated water twice and dried over magnesium sulfate (MgSO4). The organic solvent was removed by vacuum evaporation. It was then recrystalized in ethanol to obtain dithiobenzoyl disulfide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06888020B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-c850d229e6554770a472de0d406a2346 |
| Source note | uspto-grants-2005_05 |