Tri(2-ethylhexyl)amine → 5-Butoxy-4-methyl-1,3-oxazole

HRID 2184280

Reaction equation

HRID 2184280 reaction equation
[N+:1]([CH:3]([CH3:11])[C:4]([O:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:5])#[C-:2].C(C(CCCC)CN(CC(CC)CCCC)CC(CC)CCCC)C>ClC1C=CC=CC=1>[CH3:11][C:3]1[N:1]=[CH:2][O:5][C:4]=1[O:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 102705Tri(2-ethylhexyl)amineHCID 11171108n-Butyl alpha-isocyanopropionate

Product 1

HCID 98774405-Butoxy-4-methyl-1,3-oxazole

Reagents, catalysts & solvents 1

HCID 7964ChlorobenzeneSolvent

Procedure

A column according to example 1 but without a dividing wall (see FIG. 1) was continuously charged via inlet (A) with a mixture of 20.6% by weight of chlorobenzene, 5.2% by weight of n-butyl α-isocyanopropionate (R1=n-butyl, R2=methyl) and 72.60% by weight of tris(2-ethylhexyl)amine.

Sources & evidence

ORD record
ord-312a9549597e4547b328fa5943b4196a
Source dataset
uspto-grants-2005_05
Patent number
US06900332B2

Linked notes

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