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Formaldehyde → Formaldehyde, polymer with 1,3-benzenediol and phenol

HRID 2185578
Notes
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Reaction equation

HRID 2185578 reaction equation
[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].[C:9]1([OH:15])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C=O>>[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].[CH2:9]=[O:15].[C:9]1([OH:15])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 712Formaldehyde2×HCID 22639633HCID 22639633, compound

Product 1

HCID 117702Formaldehyde, polymer with 1,3-benzenediol and phenol

Procedure

A resorcinol-phenol-formaldehyde gluing system was prepared according to conventional technology by stirring 100 pans by weight of a resorcinol-phenol mixture and 20 parts by weight of an aqueous formaldehyde solution containing 40 percent by weight of formaldehyde. After said stirring the glue was applied to a surface in an amount of 400 g m2. The formaldehyde (HCHO) concentration above said surface was analysed by sucking air through a filter impregnated with dinitrophenylhydrazine, leaching the filter with acetonirile, and then analysing the extract, by means of HPLC, with regard to the content of HCHO. The volume of analysed air was 28.42 liters, which passed the filter with a flow of 0.98 liters/minute. The results of the analysis are set forth in the Table below.

Workup

concentration
The formaldehyde (HCHO) concentration above said surface
  • filtrationfilter with acetonirile, and
  • filtrationfilter with a flow of 0.98 liters/minute
  • customThe results of the analysis
  • Sources & evidence

    ORD record
    ord-7f1442632efb4dde869736792e16e996
    Source dataset
    uspto-grants-2002_06
    DOI
    10.6084/m9.figshare.5104873.v1
    Patent number
    US06402841B1

    Reaction notes

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    On this pageParticipantsProcedureWorkupSources & evidenceReaction notes