Lithium propan-2-olate → HCID 178459136, compound
Reaction equation
[CH3:1][CH:2]([CH3:4])[O-:3].[Li+:5].[CH3:6][CH:7]([CH3:9])[O-:8].[CH3:10][Ga+:11][CH3:12]>C(OCC)C>[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:10][Ga+:11][CH3:12].[Li+:5].[CH3:6][CH:7]([CH3:9])[O-:8]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
1.32 g (20.0 mmol) of lithium isopropoxide was added to 3.18 g (20.0 mmol) of dimethylgallium isopropoxide dissolved in diethyl ether and stirred for a day. The solvent was removed under a reduced pressure to obtain 3.82 g (17.0 mmol; 85% yield) of the title compound in the form of a white solid.
Workup
- customThe solvent was removed under a reduced pressure
Sources & evidence
- ORD record
- ord-3de15a7ce0b349f2b086efd3d5fc2e28
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06409830B1
Reaction notes
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