Allyl bromide → HCID 61045603, compound

HRID 2199602

Reaction equation

HRID 2199602 reaction equation
ClC1N=CC(S(NC2CCCC2)(=O)=O)=CC=1.C(Br)C=C.[Cl:21][C:22]1[N:27]=[CH:26][C:25]([S:28]([N:31]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37]C=2)[CH2:32][CH:33]=[CH2:34])(=[O:30])=[O:29])=[CH:24][CH:23]=1>>[Cl:21][C:22]1[N:27]=[CH:26][C:25]([S:28]([N:31]([CH:35]2[CH2:40][CH2:39][CH2:38][CH2:37]2)[CH2:32][CH:33]=[CH2:34])(=[O:29])=[O:30])=[CH:24][CH:23]=1

Participants

4

Reactant 3

HCID 7841Allyl bromideHCID 162273046-chloro-N-cyclopentylpyridine-3-sulfonamideHCID 244194826-chloro-N-phenyl-N-(prop-2-en-1-yl)pyridine-3-sulfonamide

Product 1

HCID 61045603HCID 61045603, compound

Procedure

According to Process 10.2, starting with 1 g of 6-chloro-N-cyclopentylpyridine-3-sulfonamide and 0.42 mL of allyl bromide, 1.2 g of 6-chloro-N-phenyl-N-(prop-2-en-1-yl)pyridine-3-sulfonamide are obtained in the form of an orange-coloured oil.

Workup

  1. customare obtained in the form of an orange-coloured oil

Sources & evidence

ORD record
ord-23594132deb14b4e9e60e4e294d88a26
Source dataset
uspto-grants-2016_06
Patent number
US09359329B2

Linked notes

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