4-Methoxy-o-phenylenediamine → [3-(6-Methoxy-1H-benzoimidazol-2-yl)-propyl]-methyl-amine

HRID 220249

Reaction equation

HRID 220249 reaction equation
COC1C=C(N)C(N)=CC=1.CO[C:13]1[C:26]([O:27][CH3:28])=[CH:25][C:16]2[NH:17][C:18]([CH2:20][CH2:21][CH2:22][NH:23][CH3:24])=[N:19][C:15]=2[CH:14]=1>>[CH3:28][O:27][C:26]1[CH:13]=[CH:14][C:15]2[N:19]=[C:18]([CH2:20][CH2:21][CH2:22][NH:23][CH3:24])[NH:17][C:16]=2[CH:25]=1

Participants

3

Reactant 2

HCID 1534044-Methoxy-o-phenylenediamineHCID 61363740[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)-propyl]-methyl-amine

Product 1

HCID 65017454[3-(6-Methoxy-1H-benzoimidazol-2-yl)-propyl]-methyl-amine

Procedure

Prepared from 4-methoxy-benzene-1,2-diamine in analogy to the methods described for [3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)-propyl]-methyl-amine.

Sources & evidence

ORD record
ord-ac7d89cfac3f4ab7b7b8b52f395e5e46
Source dataset
uspto-grants-2012_06
Patent number
US08202885B2

Linked notes

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