Benzo(B)Thiophene → 1-(Benzo[b]thiophen-2-ylmethyl)-5-bromo-2-ethoxybenzene

HRID 221072

Reaction equation

HRID 221072 reaction equation
[CH:1]1[CH:2]=[CH:3][C:4]2[S:9][CH:8]=[CH:7][C:5]=2[CH:6]=1.[Br:10][C:11]1[CH:12]=[CH:13][C:14]([O:19][CH2:20][CH3:21])=[C:15]([CH:18]=1)[CH:16]=O>>[S:9]1[C:8]([CH2:16][C:15]2[CH:18]=[C:11]([Br:10])[CH:12]=[CH:13][C:14]=2[O:19][CH2:20][CH3:21])=[CH:7][C:5]2[CH:6]=[CH:1][CH:2]=[CH:3][C:4]1=2

Participants

3

Reactant 2

HCID 7221Benzo(B)ThiopheneHCID 1449015-Bromo-2-ethoxybenzaldehyde

Product 1

HCID 666079511-(Benzo[b]thiophen-2-ylmethyl)-5-bromo-2-ethoxybenzene

Procedure

Thianaphthene and 5-bromo-2-ethoxybenzaldehyde were treated in a manner similar to Reference Example 7 to give the target compound.

Workup

  1. customto give the target compound

Sources & evidence

ORD record
ord-10b7c7baf4254201967d3e8884f99bcb
Source dataset
uspto-grants-2012_06
Patent number
US08202984B2

Linked notes

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