3-Phenylpropyl 4-methylbenzenesulfonate → 5-Phenylpentyl p-toluenesulfonate

HRID 2211078

Reaction equation

HRID 2211078 reaction equation
[CH2:1]([CH:11]1[CH2:19][C:18]2[C:13](=[CH:14][CH:15]=[C:16](C3N=CC(O)=CN=3)[CH:17]=2)C1)[CH2:2][CH2:3]CCCCCCC.C(C1C=CC(C2C=CC3C(=CC=C(O)C=3)N=2)=CC=1)CCCC.[C:49]1([CH3:68])[CH:54]=[CH:53][C:52]([S:55]([O:58]CCCC2C=CC=CC=2)(=[O:57])=[O:56])=[CH:51][CH:50]=1>>[C:49]1([CH3:68])[CH:50]=[CH:51][C:52]([S:55]([O:58][CH2:3][CH2:2][CH2:1][CH2:11][CH2:19][C:18]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)(=[O:56])=[O:57])=[CH:53][CH:54]=1

Participants

4

Reactant 3

HCID 109899213-Phenylpropyl 4-methylbenzenesulfonateHCID 193753532-(2-Decylindan-5-yl)pyrimidine-5-olHCID 21466809HCID 21466809, compound

Product 1

HCID 152495035-Phenylpentyl p-toluenesulfonateYield 58.3%

Procedure

An objective product was prepared in the same manner as in Example 2 except that 2-(2-decylindan-5-yl)pyrimidine-5-ol was changed to 2-(4-pentylphenyl)quinoline-6-ol and 3-phenylpropyl p-toluenesulfonate was changed to 5-phenylpentyl p-toluenesulfonate (Yield: 58.3%).

Sources & evidence

ORD record
ord-31c08ab87a394db8bbb9cde4860dc0e0
Source dataset
uspto-grants-1995_10
Patent number
US05462694

Linked notes

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