cis-4-Methylcyclohexylammonium chloride → HCID 178461400, compound
Reaction equation
[Cl-:1].[CH3:2][CH:3]1[CH2:8][CH2:7][CH:6]([NH3+:9])[CH2:5][CH2:4]1>C(Cl)Cl>[Cl-:1].[CH3:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([NH3+:9])[CH2:5][CH2:4]1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
4-methylcyclohexylammonium chloride (Example 71) was suspended in 4 ml of methylene chloride cooled. The crystal obtained was filtered out, yielding 3.2 g of trans-4-methylcyclohexylammonium chloride as white crystal, which had the following physiochemical properties:
Workup
- temperaturecooled
- customThe crystal obtained
- filtrationwas filtered out
Sources & evidence
- ORD record
- ord-a8cc399b69e8417d9d90b9d15e0ce362
- Source dataset
- uspto-grants-1994_09
- Patent number
- US05344845
Reaction notes
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