HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 4-(phenylmethyl)- → (4-Benzyl-phenyl)-(2-methyl-6-nitro-phenyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 4-(phenylmethyl)- | HCID 136914 | — |
| Reactant | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | (4-Benzyl-phenyl)-(2-methyl-6-nitro-phenyl)-amine | HCID 68834454 | — |
Reaction Steps
The product (1.01 g) is obtained according to the method of stage 1 of Example 4, by using 1.13 g of 2-fluoro-3-methyl-nitrobenzene and 2 g of 4-benzyl-aniline in the presence of 1.31 g of potassium tert-butanolate in 30 mL of DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207373B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-d458c972e6344078914415d4be3fddfb |
| Source note | uspto-grants-2012_06 |