Ammonia → N-(2,4,6-tribromophenyl)glycinamide
Reaction equation
[Br:1][C:2]1[CH:7]=[C:6]([Br:8])[CH:5]=[C:4]([Br:9])[C:3]=1NCC(OCC)=O.C1([NH:23][CH2:24][C:25](OCC)=[O:26])C=CC=CC=1.BrBr.[NH3:32]>O.C(O)(=O)C.C(O)C>[Br:1][C:2]1[CH:3]=[C:4]([Br:9])[CH:5]=[C:6]([Br:8])[C:7]=1[NH:32][C:25](=[O:26])[CH2:24][NH2:23]Participants
8
Reactant 4
Product 1
Reagents, catalysts & solvents 3
Procedure
The ester required for Id, ethyl N-(2,4,6-tribromophenyl)glycinate (IV), was prepared by the reaction of ethyl N-phenylglycinate with bromine in a mixture of water and acetic acid. IV reacted with ammonia in ethanol solution to form N-(2,4,6-tribromophenyl)glycinamide (V).
Sources & evidence
- ORD record
- ord-12a572969296471cbfd69e364352926a
- Source dataset
- uspto-grants-1982_10
- Patent number
- US04352930
Reaction notes
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