3-Bromo-4-fluoroaniline → HCID 58945795, compound

Reaction equation

[N+:1](=[C:3]1[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]1=[O:10])=[N-].[Br:11][C:12]1[CH:13]=[C:14]([CH:16]=[CH:17][C:18]=1[F:19])N>>[Br:11][C:12]1[CH:13]=[C:14]([N:1]([C:3]2[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]=2[OH:10])[C:3]2[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]=2[OH:10])[CH:16]=[CH:17][C:18]=1[F:19]

Participants

Reactant 2

HCID 27792863-Bromo-4-fluoroaniline

HCID 110624492-Diazocyclohexane-1,3-dione

Product 1

HCID 58945795HCID 58945795, compound

Procedure

Following the procedure described in the Example 1, using 2-diazo-cyclohexane-1,3-dione and 3-bromo-4-fluoroaniline as starting materials to yield the title compound as a white solid.

Sources & evidence

ORD record: ord-22834ac9aab64ac9ad54f672b2bad03b
Source dataset: uspto-grants-2010_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07674793B2

Reaction notes

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