Myristic Acid → Tetradecanoic acid, strontium salt (2:1)

HRID 225034

Reaction equation

HRID 225034 reaction equation
[C:1]([OH:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].O.O.O.O.O.O.O.O.[OH-].[Sr+2:26].[OH-]>O>[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Sr+2:26].[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 2

HCID 11005Myristic AcidHCID 21617461Strontium hydroxide octahydrate

Product 1

HCID 167169Tetradecanoic acid, strontium salt (2:1)

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
50 °C

Procedure

100 of myristic acid which has been granulated from an aqueous emulsion as described in Example 1 (AN 246, titer 53° C. particle size 0.2-0.3 mm.) and 60.2 g strontium hydroxide octahydrate (97% active) are suspended in one liter of water at 50° C. temperature and stirred for 30 minutes at 50° C. followed by 60 minutes of agitation at 70° C. The hollow formed granulate is filtered and dried. The content of free fatty acid amounts to 1.7%.

Workup

  1. customtiter 53° C.
  2. waitfollowed by 60 minutes of agitation at 70° C
  3. filtrationThe hollow formed granulate is filtered
  4. customdried

Sources & evidence

ORD record
ord-0e0c9f328fc14207a0f5b0bbce5340c2
Source dataset
uspto-grants-1980_11
Patent number
US04235794

Linked notes

Loading…