Dihydro-2-methyl-3(2H)-furanone → HCID 57753356, compound

HRID 225636

Reaction equation

HRID 225636 reaction equation
[CH2:1]([N:8]1[CH2:16][C:15]2[C:10](=[CH:11][CH:12]=[C:13](Br)[CH:14]=2)[CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:18][CH:19]1[C:23](=[O:24])[CH2:22][CH2:21][O:20]1>>[CH2:1]([N:8]1[CH2:16][C:15]2[C:10](=[CH:11][CH:12]=[C:13]([C:23]3([OH:24])[CH2:22][CH2:21][O:20][CH:19]3[CH3:18])[CH:14]=2)[CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 18522Dihydro-2-methyl-3(2H)-furanoneHCID 534165502-Benzyl-5-bromo-2,3-dihydro-1H-isoindole

Product 1

HCID 57753356HCID 57753356, compound

Procedure

Prepared in analogy to Example A62(b) from 2-benzyl-5-bromo-2,3-dihydro-1H-isoindole (Example A62(a)) and 2-methyltetrahydrofuran-3-one. Brown oil. MS (m/e): 310.4 ([M+H]+, 100%).

Sources & evidence

ORD record
ord-4baba0cfaf484de289598c3431c5d523
Source dataset
uspto-grants-2009_07
Patent number
US07557114B2

Linked notes

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