Sodium Hydroxide → Isotridecanoic acid

HRID 2256421Notes

Reaction equation

HRID 2256421 reaction equation
[CH2:1]([OH:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]([CH3:13])[CH3:12].[OH-:15].[Na+]>>[C:1]([OH:15])(=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH:11]([CH3:12])[CH3:13]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 33865Isotridecan-1-ol

Product 1

HCID 33002Isotridecanoic acid

Conditions

Temperature
340 °C

Procedure

180 kg of isotridecyl alcohol and 33.6 kg of NaOH were introduced into the 350 liter reactor and heated to 340° C. under a nitrogen pressure of 6 bar. The process was otherwise carried out as described in Example 1. The product obtained had an acid value of 240 and an OH value of 6.3.

Workup

  1. customThe product obtained

Sources & evidence

ORD record
ord-f441da02fbca4202b1a3755c32f10e74
Source dataset
uspto-grants-1997_08
Patent number
US05654453

Reaction notes

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