2-Mercaptoethanol → 2-[{3-(1,3-Benzodioxol-5-yl)propyl}dithio]ethanol

HRID 2259769

Reaction equation

[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH2:11][CH2:12][SH:13])=[CH:9][C:4]=2[O:3][CH2:2]1.[SH:14][CH2:15][CH2:16][OH:17]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH2:11][CH2:12][S:13][S:14][CH2:15][CH2:16][OH:17])=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

Reactant 2

HCID 15672-Mercaptoethanol

HCID 190016193-(1,3-Dioxaindan-5-yl)propane-1-thiol

Product 1

HCID 190016282-[{3-(1,3-Benzodioxol-5-yl)propyl}dithio]ethanolYield 43.8%

Procedure

8.4 g of the title compound was prepared from 27.8 g 3-(1,3-benzodioxol-5-yl)propanethiol and 5.5 g of 2-mercaptoethanol as a colorless oil according to the same procedure as that described in Example 1.

Sources & evidence

ORD record: ord-35e32022554846e490672d77a7995afc
Source dataset: uspto-grants-1995_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05475024

Linked notes

Loading…