6-Methoxy-2-methylbenzothiazole → 2-Methyl-1,3-benzothiazol-6-ol

HRID 22705

Reaction equation

HRID 22705 reaction equation
C[O:2][C:3]1[CH:12]=[CH:11][C:6]2[N:7]=[C:8]([CH3:10])[S:9][C:5]=2[CH:4]=1.CC1SC2C=C(OCC3CO3)C=CC=2N=1>>[CH3:10][C:8]1[S:9][C:5]2[CH:4]=[C:3]([OH:2])[CH:12]=[CH:11][C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 762546-Methoxy-2-methylbenzothiazoleHCID 225916342-Methyl-6-(oxiran-2-ylmethoxy)benzothiazole

Product 1

HCID 7593042-Methyl-1,3-benzothiazol-6-ol

Procedure

Compound 50 was prepared from the commercially available 6-methoxy-2-methyl-benzothiazole as described in partC-4 of Example 1. Synthesis of 2-methyl-6-(oxiran-2-ylmethoxy)benzothiazole (51):

Sources & evidence

ORD record
ord-938449baeb154a4ea64092e88bf4c2b0
Source dataset
uspto-grants-2005_02
Patent number
US06849632B2

Linked notes

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