Ethylene butyl acrylate → Butyl Acrylate

Reaction equation

C([O-])(=O)CCCCCCCCCCC.C([Sn+2]CCCCCCCC)CCCCCCC.C([O-])(=O)CCCCCCCCCCC.[C:46]([O:50][CH2:51][CH2:52][CH2:53][CH3:54])(=[O:49])[CH:47]=[CH2:48].C=C>>[C:46]([O:50][CH2:51][CH2:52][CH2:53][CH3:54])(=[O:49])[CH:47]=[CH2:48]

Participants

Reactant 2

HCID 16212797Ethylene butyl acrylate

HCID 22292224Dioctyltin laurate

Product 1

HCID 8846Butyl Acrylate

Procedure

Master batch of catalyst: The master batch was prepared by impregnating of dioctyltin laurate to pellets of a conventional ethylene butyl acrylate copolymer produced in a high pressure in a tubular reactor (butyl acrylate, BA, content 15 wt %) as the carrier polymer. The obtained master batch contained 3.5 wt % of the catalyst based on the final amount of the master batch. Inventive Master Batches 1 to 7: Inventive Catalyst 1:

Workup

customMaster batch of catalyst: The master batch was prepared

Sources & evidence

ORD record: ord-79d62fe24c4341a38254cf886678c755
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09133331B2

Reaction notes

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