HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → 3-[3-(2,6-Dimethylphenylamino)-6-nitroimidazo[1,2-a]pyridin-2-yl]-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | 2,6-Dimethylphenyl isocyanide | HCID 76009 | — |
| Reactant | 2-Amino-5-nitropyridine | HCID 77888 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | 3-[3-(2,6-Dimethylphenylamino)-6-nitroimidazo[1,2-a]pyridin-2-yl]-phenol | HCID 9864361 | — |
Reaction Steps
Compound (12) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-5-nitropyridine solution (0.1 M, DCM), 0.575 ml of 2,6-dimethylphenyl isocyanide solution (0.2 M, DCM), 0.500 ml of 3-hydroxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-b197a4e0af4c4b9296dbdbdd21df01ff |
| Source note | uspto-grants-2005_02 |