HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 69731780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Reactant | Methyl isocyanoacetate | HCID 547815 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 69731780 | HCID 69731780 | — |
Reaction Steps
Compound (31) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of methyl isocyanoacetate solution (0.2 M, DCM), 0.500 ml of acetaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-cf3f0544354a4906b653eb322f8d020a |
| Source note | uspto-grants-2005_02 |