HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl isocyanate → HCID 178418561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 3-[4-(4-Chlorobenzyl)homopiperazin-1-yl]-propanethiol | HCID 20153174 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418561 | HCID 178418561 | 77.6% |
Reaction Steps
The procedure described in Example 2 was followed, using 1.3 g of n-hexyl isocyanate, 3.0 g of 3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propanethiol and 75 ml of methylene chloride, to give 1.3 g (33% of theory) of N-(n-hexyl)-S-{3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propyl}thiocarbamate dihydrochloride as a tan powder, M.p. 183°-187° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618677 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-997e1d6449954340b4d905cb9ec92291 |
| Source note | uspto-grants-1986_10 |