2,2,2-Trichloroethyl chloroformate → HCID 13936026, compound
Reaction equation
Cl[C:2](Cl)(Cl)[CH2:3]OC(Cl)=O.[OH:10][CH:11]1[C:16](=[O:17])[NH:15][C:14]([CH3:18])=[CH:13][S:12]1>N1C=CC=CC=1>[OH:10][CH:11]1[C:16](=[O:17])[NH:15][C:14]([CH3:18])=[C:13]([C:3]2[CH:2]=[CH:16][N:15]=[CH:14][CH:13]=2)[S:12]1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A mixture of pyridine, 2,2,2-trichloroethylchloroformate and 2-hydroxy-5-methyl-2H-1,4-thiazin-3(4H)-one was treated in the same manner as described in Example 6. The residue was recrystallized from ethanol to give the titled compound as pale yellow crystals.
Workup
- additionwas treated in the same manner
- customThe residue was recrystallized from ethanol
Sources & evidence
- ORD record
- ord-6b540a8a25874b919febac7cbf4703b6
- Source dataset
- uspto-grants-1989_01
- Patent number
- US04800201
Reaction notes
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