HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Tert-butyl-4-methoxybenzoyl chloride → Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Tert-butyl-4-methoxybenzoyl chloride | HCID 13633555 | — |
| Reactant | Allyl 4-hydroxymethyl-2-hydroxybenzoate | HCID 21474558 | — |
| Product | Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate | HCID 21474526 | — |
Reaction Steps
In a manner similar to Example 1(d), by reaction of 2.4 g (10.5 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 2.2 g (10.5 mmol) of allyl 4-hydroxymethyl-2-hydroxybenzoate, 2.5 g (61%) of the expected allyl ester are obtained in the form of a slightly yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688817 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-3fd2230ffb6d4043807846fb672aac58 |
| Source note | uspto-grants-1997_11 |