p-Fluoronitrobenzene → HCID 20031356, compound
Reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH2:11]([N:14]1[CH2:20][CH2:19][CH2:18][NH:17][CH2:16][CH2:15]1)[CH2:12][CH3:13]>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([N:17]2[CH2:18][CH2:19][CH2:20][N:14]([CH2:11][CH2:12][CH3:13])[CH2:15][CH2:16]2)=[CH:3][CH:4]=1)([O-:10])=[O:9]Participants
3
Procedure
In a manner similar to Preparation 2, react 1-fluoro-4-nitrobenzene with hexahydro-1-propyl-1H-1,4-diazepine to obtain the title compound.
Workup
- customIn a manner similar to Preparation 2
Sources & evidence
- ORD record
- ord-5459cea5cbd44ed6ac9aa75813b6f8ff
- Source dataset
- uspto-grants-1989_07
- Patent number
- US04851526
Reaction notes
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