Ammonium Chloride → HCID 178419899, compound
Reaction equation
[C:1]([CH2:3][S:4][CH:5]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[CH2:9][O:8][C:7]2[CH:16]=[CH:17][C:18]([O:20][CH2:21][C:22]3[CH:31]=[CH:30][C:29]4[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=4)[N:23]=3)=[CH:19][C:6]1=2)#[N:2].[Cl-].[NH4+].[N-:34]=[N+:35]=[N-:36].[Na+]>>[N:23]1[C:24]2[C:29](=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH:30]=[CH:31][C:22]=1[CH2:21][O:20][C:18]1[CH:17]=[CH:16][C:7]2[O:8][CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]([S:4][CH2:3][C:1]3[NH:36][N:35]=[N:34][N:2]=3)[C:6]=2[CH:19]=1Participants
4
Procedure
11-Cyanomethylthio-2-(quinolin-2-yl)methoxy-6,11-dihydrodibenz[b,e]oxepine, ammonium chloride and sodium azide were used and reacted in the same manner as in Example 32 to obtain the title compound.
Workup
- customreacted in the same manner as in Example 32