4-Ethoxy-2,3-difluorobenzoic acid → HCID 178455402, compound

HRID 234558

Reaction equation

HRID 234558 reaction equation
[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([OH:10])=[O:9])=[C:6]([F:13])[C:5]=1[F:14])[CH3:2].[C:15]1([Si:21]2(CCCC)[CH2:26][CH2:25][CH:24]([CH:27]3[CH2:32][CH2:31][CH:30](O)[CH2:29][CH2:28]3)[CH2:23][CH2:22]2)C=C[CH:18]=[CH:17][CH:16]=1>>[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([O:10][C@H:30]2[CH2:29][CH2:28][C@H:27]([CH:24]3[CH2:23][CH2:22][SiH:21]([CH2:15][CH2:16][CH2:17][CH3:18])[CH2:26][CH2:25]3)[CH2:32][CH2:31]2)=[O:9])=[C:6]([F:13])[C:5]=1[F:14])[CH3:2]

Participants

3

Reactant 2

HCID 27694004-Ethoxy-2,3-difluorobenzoic acidHCID 233548284-(4-Phenyl-4-n-butyl-4-silacyclohexyl)cyclohexanol

Product 1

HCID 178455402HCID 178455402, compound

Procedure

The general procedure of Example 31 was repeated using 4-ethoxy-2,3-difluorobenzoic acid and 4-(4-phenyl-4-n-butyl-4-silacyclohexyl)cyclohexanol, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-d586d7f570cb4d5589f86442a6e1173f
Source dataset
uspto-grants-1997_01
Patent number
US05595686

Linked notes

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