HCID 19705058, compound → HCID 23353545, compound

Reaction equation

CN(C)[C:3]1[N:8]=[C:7]([NH2:9])[C:6]([C:10]2[CH:15]=[CH:14][C:13]([Cl:16])=[CH:12][C:11]=2[Cl:17])=[CH:5][N:4]=1.S(O)(O)(=O)=O.[N:24]1(C(N)=N)[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1>>[NH:24]1[CH2:29][CH2:28][CH2:27][CH2:26][CH:25]1[C:3]1[N:8]=[C:7]([NH2:9])[C:6]([C:10]2[CH:15]=[CH:14][C:13]([Cl:16])=[CH:12][C:11]=2[Cl:17])=[CH:5][N:4]=1

Participants

Reactant 2

HCID 19705058HCID 19705058, compound

HCID 20561340HCID 20561340, compound

Product 1

HCID 23353545HCID 23353545, compound

Procedure

This compound was prepared in an analogous manner to the compound of Example 76 from 1-piperidinecarboxamidine sulphate (Bader), mp. 169° C.

Sources & evidence

ORD record: ord-731ca2aa10e44cffa66be3b392c1ff44
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05597827

Reaction notes

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