Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
Reaction equation
[CH3:1][C@H]1OC(=O)C2C(O)=CC(O)=C(Cl)C=2CC(=O)C=CC=C[C@H]2O[C@H]2C1.C(O)(=O)CCCCCCC/C=C\CCCCCC.[CH:44]1([N:50]=[C:51]=[N:52][CH:53]2[CH2:58][CH2:57][CH2:56]CC2)CCCCC1>C(Cl)Cl>[CH3:1][N:50]([C:51]1[CH:56]=[CH:57][CH:58]=[CH:53][N:52]=1)[CH3:44]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 636 mg of palmitoleic acid, 20 ml of dry methylene chloride, 716 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 654 mg of the title compound were obtained.
Sources & evidence
- ORD record
- ord-ec2419e8589248568d4d5df51945cc8a
- Source dataset
- uspto-grants-1997_01
- Patent number
- US05597846
Reaction notes
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