Ethylenediamine → HCID 14651800, compound
Reaction equation
[C:1]([C:3]([CH3:13])([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:4])#[N:2].[CH2:14](N)[CH2:15][NH2:16]>C(=S)=S>[CH3:4][C:3]([C:1]1[NH:2][CH2:14][CH2:15][N:16]=1)([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:13]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
18.32 g (100 mmoles) of 2-cyano-2-methyldecane, 8.5 ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 13.91 g (62%) of the product.
Workup
- distillationDistillation of the residue
Sources & evidence
- ORD record
- ord-bdba5c0bbe55404592e9833eca563d7c
- Source dataset
- uspto-grants-1989_10
- Patent number
- US04876249
Reaction notes
Loading…