Water → 1-Butanaminium, N,N,N-trimethyl-, hydroxide (1:1)
Reaction equation
[I-].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7].[OH2:10]>[Ag-]=O>[OH-:10].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A typical TMBAOH solution was prepared as follows. Trimethylbutylammonium iodide, 1466.3 g, was dissolved in 1948.6 g deionized water in a 5 liter 3-necked round bottom flask equipped with overhead stirring. A 1 wt. % excess of silver(I) oxide, (99%), 712 g, was added and stirred in the dark for 24 hours. The resulting trimethylbutylammonium hydroxide solution was isolated by filtration.
Workup
- customA typical TMBAOH solution was prepared
- customequipped with overhead stirring
Sources & evidence
- ORD record
- ord-23715dcbdede4dc590d48a73f736771d
- Source dataset
- uspto-grants-2010_07
- Patent number
- US07763764B2
Reaction notes
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