Propanoic acid, 2-bromo-2-methyl-, ethyl ester → HCID 178431962, compound

Reaction equation

[CH:1]1([CH2:7][NH:8][C:9]([NH2:11])=[S:10])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Br[C:13]([CH3:20])([CH3:19])[C:14](OCC)=[O:15]>>[CH:1]1([CH2:7][NH:8][C:9]2[S:10][C:13]([CH3:20])([CH3:19])[C:14](=[O:15])[N:11]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 2

HCID 11745Propanoic acid, 2-bromo-2-methyl-, ethyl ester

HCID 11829924Cyclohexylmethyl-thiourea

Product 1

HCID 178431962HCID 178431962, compound

Procedure

Synthesis was performed from N-(cyclohexylmethyl)thiourea and ethyl 2-bromoisobutyrate according to Method C.

Workup

customSynthesis

Sources & evidence

ORD record: ord-da431fe8f3aa480b8bbc32aae706dc4d
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08686011B2

Reaction notes

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