Sodium Hydroxide → (2-Bromophenyl)hydrazine

HRID 2360490

Reaction equation

HRID 2360490 reaction equation
Cl.[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10].[OH-].[Na+]>C1(C)C=CC=CC=1>[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 27239122-Bromophenylhydrazine hydrochloride

Product 1

HCID 85583(2-Bromophenyl)hydrazine

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

15 g 2-bromophenylhydrazine hydrochloride are suspended in 400 ml of toluene and combined with 240 ml of 1 N sodium hydroxide solution. The mixture is stirred for 1 hour and the phases are separated. The organic phase is dried on magnesium sulphate and the solvents are eliminated in vacuo. The crude product thus obtained is further reacted directly.

Workup

  1. customthe phases are separated
  2. customThe organic phase is dried on magnesium sulphate

Sources & evidence

ORD record
ord-15172afbc4084c749fa1d4454ea24d19
Source dataset
uspto-grants-2014_04
Patent number
US08686022B2

Linked notes

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