HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxybenzeneacetonitrile → (Z)-2-(3,4-dimethoxy-phenyl)-3-phenanthren-9-yl-acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Reactant | Phenanthrene-9-carbaldehyde | HCID 78437 | — |
| Product | (Z)-2-(3,4-dimethoxy-phenyl)-3-phenanthren-9-yl-acrylonitrile | HCID 11964784 | 63% |
Reaction Steps
Phenanthrene-9-aldehyde (250 mg) was condensed with 3,4-dimethoxybenzyl cyanide (214 mg) through Method A (production step 2), to thereby yield the target product (yield: 278 mg, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697742B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-6fae2bfe641e4e7e920b97f5be6c9f0d |
| Source note | uspto-grants-2014_04 |