Hydrazine → 2-Hydrazinyl-4,8-dimethylquinoline

HRID 2368696

Reaction equation

HRID 2368696 reaction equation
Cl[C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1.[NH2:14][NH2:15]>>[NH:14]([C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1)[NH2:15]

Participants

3

Reactant 2

HCID 9321HydrazineHCID 2691612-Chloro-4,8-dimethylquinoline

Product 1

HCID 36843162-Hydrazinyl-4,8-dimethylquinoline

Procedure

A solution of 2-chloro-4,8-dimethylquinoline (1.00 g, 5.2 mmoles) in NH2NH2 was reacted as outlined in Scheme 1 above to give the desired title compound which was used in the next step without further purification.

Sources & evidence

ORD record
ord-89281aec8c8c4071916dd632eefe7626
Source dataset
uspto-grants-2014_04
Patent number
US08703797B2

Linked notes

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