Dibutyltin dilaurate → 1-Ethyl-2,3-dimethylimidazolium acetate

Reaction equation

[C:1]([O-:4])(=[O:3])[CH3:2].[CH2:5]([N+:7]1[CH:11]=[CH:10][N:9]([CH2:12]C)[CH:8]=1)[CH3:6].[C:14]([O-])(=O)CCCCCCC.C([N+]1C=CN(CC)C=1)C.CCCCCCCCCCCC(O[Sn](OC(CCCCCCCCCCC)=O)(CCCC)CCCC)=O>>[C:1]([O-:4])(=[O:3])[CH3:2].[CH2:5]([N+:7]1[CH:11]=[CH:10][N:9]([CH3:12])[C:8]=1[CH3:14])[CH3:6]

Participants

Reactant 3

HCID 16682738Dibutyltin dilaurate

HCID 866734861H-Imidazolium, 1,3-diethyl-, acetate (1:1)

HCID 866734871,3-Diethylimidazolium octanoate

Product 1

HCID 1784763801-Ethyl-2,3-dimethylimidazolium acetate

Procedure

1,3-diethylimidazolium acetate and 1,3-diethylimidazolium octanoate are better relative to DBTL as reference, in terms of drying and the early development of pendulum hardness.

Workup

customof drying

Sources & evidence

ORD record: ord-9b27754324ad4a5eb69a08642eed1ffc
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08709544B2

Reaction notes

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