Sodium Azide → HCID 178527644, compound

Reaction equation

[S:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][NH:15][C:16](=[S:19])SC)([OH:4])(=[O:3])=[O:2].[N-:20]=[N+:21]=[N-:22].[Na+]>>[S:1]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][N:15]1[C:16]([SH:19])=[N:22][N:21]=[N:20]1)([OH:4])(=[O:3])=[O:2]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 2131509810-{[(Methylsulfanyl)carbonothioyl]amino}decane-1-sulfonic acid

Product 1

HCID 178527644HCID 178527644, compound

Procedure

Methyl 10-sulfodecyldithiocarbamate (31.4 g., 0.096 mol.) is reacted with 6.5 g. (0.1 mol.) of sodium azide as described above to give 1-(10-sulfodecyl)tetrazole-5-thiol.

Sources & evidence

ORD record: ord-dc7f08fcf3f04c0080e3d2f9a1abbb76
Source dataset: uspto-grants-1979_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04159373

Reaction notes

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