HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cinnamyl bromide → 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cinnamyl bromide | HCID 5357478 | — |
| Reactant | 4-Ethyl-4-(5-fluoro-3-hydroxyphenyl)-2,2-dimethyl-1,3-dioxolane | HCID 19088699 | — |
| Product | 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane | HCID 19756609 | 2% |
Reaction Steps
Using the procedure described in Example 6, (E)-cinnamyl bromide was reacted with 4-ethyl-4-(5-fluoro-3-hydroxyphenyl)-2,2-dimethyl-1,3-dioxolane to give 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane in 2% yield, as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05098932 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-f84fd097ddd948408e3211658c764c83 |
| Source note | uspto-grants-1992_03 |