Ethyl bromoacetate → Ethyl (2,3,5-trimethylphenoxy)acetate

Reaction equation

[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1[OH:10].[CH2:11]([O:13][C:14](=[O:17])[CH2:15]Br)[CH3:12]>>[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1[O:10][CH2:15][C:14]([O:13][CH2:11][CH3:12])=[O:17]

Participants

Reactant 2

HCID 7748Ethyl bromoacetate

HCID 127692,3,5-Trimethylphenol

Product 1

HCID 28940153Ethyl (2,3,5-trimethylphenoxy)acetate

Procedure

Using 2,3,5-trimethylphenol and ethylbromoacetate, the title compound was synthesized in the same manner as in Reference Example 153. Yield: quantitative. Oily matter.

Sources & evidence

ORD record: ord-49833f0b71f34467852c72e7a8dd8608
Source dataset: uspto-grants-2008_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07465815B2

Reaction notes

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