Dimethyl-2,6-naphthalenedicarboxylate → 2,6-Naphthalenedicarboxylic acid

HRID 2380

Reaction equation

HRID 2380 reaction equation
C[O:2][C:3]([C:5]1[CH:14]=[CH:13][C:12]2[C:7](=[CH:8][CH:9]=[C:10]([C:15]([O:17]C)=[O:16])[CH:11]=2)[CH:6]=1)=[O:4]>[Ti]>[CH:11]1[C:12]2[C:7](=[CH:6][C:5]([C:3]([OH:4])=[O:2])=[CH:14][CH:13]=2)[CH:8]=[CH:9][C:10]=1[C:15]([OH:17])=[O:16]

Participants

3

Reactant 1

HCID 61225Dimethyl-2,6-naphthalenedicarboxylate

Product 1

HCID 143572,6-Naphthalenedicarboxylic acid

Reagents, catalysts & solvents 1

HCID 23963TitaniumCatalyst

Procedure

The hydrolysis of dimethyl-2,6-naphthalenedicarboxylate was conducted in the batch-mode in a 2 liter, stirred, titanium-lined reactor. The reaction time, temperature, pressure and analysis of the resulting 2,6-naphthalenedicarboxylic acid are provided in Table 5.

Sources & evidence

ORD record
ord-558175fef481481a9e6bb6eb3ef92dfd
Source dataset
uspto-grants-1998_03
Patent number
US05728870

Linked notes

Loading…