HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2387Generated: October 26, 2026
Allylamine → N-allyl-3-(N-vinylformamido)propionamide
https://huagongshe.com/reaction/2387
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | ethyl 3-(N-vinylformamido)propionate | HCID 19690337 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-allyl-3-(N-vinylformamido)propionamide | HCID 19690345 | — |
Reaction Steps
A 100mL stainless steel high pressure reactor was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 5.7 grams (0.1 mol) of allylamine and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was heated at 90° C. for 3 hours. Subsequent NMR analysis of the reaction mixture showed no conversion of the starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05728878 |
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| Source dataset | uspto-grants-1998_03 |
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| ORD ID | ord-e627c68d0c1743fc987ec32e90fb2b64 |
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| Source note | uspto-grants-1998_03 |
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