HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | Pyruvic aldehyde dimethyl acetal | HCID 80650 | — |
| Product | N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine | HCID 71380533 | — |
Reaction Steps
12.9 mL 1,1-dimethoxyacetone was added to 10 mL benzylamine in 100 mL petrolether. Magnesiumsulfate was added and the reaction was stirred over night at RT. The mixture was filtered and evaporated to give 18.9 g of the desired product. (M+H)+: 209
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642774B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-b3bc05dd952240c8a50ff875b993000c |
| Source note | uspto-grants-2014_02 |