1H-1,2,4-Triazole → 1-(4-Nitrophenyl)-1H-1,2,4-triazole

Reaction equation

F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[NH:11]1[CH:15]=[N:14][CH:13]=[N:12]1>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([N:11]2[CH:15]=[N:14][CH:13]=[N:12]2)=[CH:3][CH:4]=1)([O-:10])=[O:9]

Participants

Reactant 2

HCID 92571H-1,2,4-Triazole

HCID 9590p-Fluoronitrobenzene

Product 1

HCID 110953981-(4-Nitrophenyl)-1H-1,2,4-triazole

Procedure

The title compound was prepared from 4-fluoronitrobenzene (2 g) and 1,2,4-triazole (1 g) as described in Description 61 to give a white solid (2.6 g, 97%).

Sources & evidence

ORD record: ord-8554e3fb88f14ded9e7a03685701f533
Source dataset: uspto-grants-1998_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05801170

Reaction notes

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