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Potassium Hydroxide → HCID 131720829, compound

HRID 2393684
Notes
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Reaction equation

HRID 2393684 reaction equation
[OH-:1].[K+:2].[CH:3]([CH:9]1[CH2:14][C:13](=[O:15])[O:12][C:10]1=[O:11])=[CH:4][CH2:5][CH2:6][CH2:7][CH3:8]>C(O)CO>[K+:2].[K+:2].[CH:3]([CH:9]([CH2:14][C:13]([O-:12])=[O:15])[C:10]([O-:1])=[O:11])=[CH:4][CH2:5][CH2:6][CH2:7][CH3:8]
ParticipantsConditionsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 148309HCID 148309, compound

Product 1

HCID 131720829HCID 131720829, compound

Reagents, catalysts & solvents 1

HCID 174Ethylene GlycolSolvent

Conditions

Temperature
100 °C

Procedure

Into a glass flask there were charged 16 grams of potasium hydroxide, 41.5 grams of ethyleneglycol and 25.5 grams of hexenyl succinic anhydride. The mixture was stirred for two hours at 100° C. Yield: 78.9 grams=98.0% of theoretical. The catalyst solution thus obtained is hygroscopic.

Workup

  1. customThe catalyst solution thus obtained

Sources & evidence

ORD record
ord-ca4ad8775782427aa2e8ccacc2878e88
Source dataset
uspto-grants-1998_09
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US05807958

Reaction notes

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On this pageParticipantsConditionsProcedureWorkupSources & evidenceReaction notes