HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-4-carboxaldehyde → 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-4-carboxaldehyde | HCID 333703 | — |
| Reactant | 2-(2-Thienyl)ethyl methanesulphonate | HCID 3047723 | — |
| Product | 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde | HCID 18973449 | 39.1% |
Reaction Steps
The same procedures used in Example 1 were repeated except for using 435 mg of indole-4-carbaldehyde and 680 mg of 2-(thien-2-yl)ethyl methanesulfonate instead of the benzyl bromide used in Example 1 to give 299 mg of 1-[2-(thien-2-yl)ethyl]indole-4-carbaldehyde as an orange-colored oily substance. The yield thereof was found to be 39%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811439 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-4573cf993a3f4246baa35f49df38e063 |
| Source note | uspto-grants-1998_09 |